Tert-Butyl 4-(bromomethyl)phenylcarbamate
- Product Name
- Tert-Butyl 4-(bromomethyl)phenylcarbamate
- CAS No.
- 239074-27-2
- Chemical Name
- Tert-Butyl 4-(bromomethyl)phenylcarbamate
- Synonyms
- tert-Butyl (4-(bromomethyl);N-Boc-4-(broMoMethyl)aniline;TERT-BUTYL 4-(BROMOMETHYL)PHENYLCARBAMATE;tert-butyl N-[4-(bromomethyl)phenyl]carbamate;4-(1,1-dimethylethoxycarbonylamino)benzylbromide;(4-Bromomethyl)phenyl]carbamic acid tert-butyl ester;Carbamic acid, [4-(bromomethyl)phenyl]-, 1,1-dimethylethyl e...;Carbamic acid, [4-(bromomethyl)phenyl]-, 1,1-dimethylethyl ester;Carbamic acid, N-[4-(bromomethyl)phenyl]-, 1,1-dimethylethyl ester
- CBNumber
- CB62459172
- Molecular Formula
- C12H16BrNO2
- Formula Weight
- 286.16
- MOL File
- 239074-27-2.mol
Tert-Butyl 4-(bromomethyl)phenylcarbamate Property
- Boiling point:
- 309.7±25.0 °C(Predicted)
- Density
- 1.376±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 13.49±0.70(Predicted)
Safety
- HS Code
- 2921490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- B201058
- Product name
- N-Boc-4-(Bromomethyl)aniline
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- J55812
- Product name
- tert-Butyl4-(bromomethyl)phenylcarbamate
- Packaging
- 1g
- Price
- $115
- Updated
- 2021/12/16
- Product number
- 7355AJ
- Product name
- tert-Butyl4-(bromomethyl)phenylcarbamate
- Packaging
- 1g
- Price
- $151
- Updated
- 2021/12/16
- Product number
- HCH0373079
- Product name
- TERT-BUTYL-4-(BROMOMETHYL)PHENYLCARBAMATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.97
- Updated
- 2021/12/16
- Product number
- CD12092937
- Product name
- tert-Butyl(4-(bromomethyl)phenyl)carbamate
- Purity
- 95%
- Packaging
- 10g
- Price
- $559
- Updated
- 2021/12/16
Tert-Butyl 4-(bromomethyl)phenylcarbamate Chemical Properties,Usage,Production
Synthesis
To a 1 L round bottom flask was added (4-hydroxymethyl-phenyl)-carbamic acid tert-butyl ester (22.3 g, 0.10 mol) obtained from Examples 2pp through 2ooo, Step 1, dichloromethane (400 mL) and triphenylphospine (31.5 g, 0.12 mol). Upon cooling to 0 °C, N-bromosuccinimide (19.6 g, 0.11 mmol) was added in small portions, and the reaction was allowed to warm to room temperature and stirred under nitrogen for 1 h. The mixture was transferred into a large flask, and hexanes were added until the solution became turbid. The solution was eluted through a plug of silica (300 g) with 1:9 ethyl acetate: hexanes and concentrated to yield Tert-Butyl 4-(bromomethyl)phenylcarbamate (12.8 g, 0.057 mol, 57 percent) as a white solid.
Tert-Butyl 4-(bromomethyl)phenylcarbamate Preparation Products And Raw materials
Raw materials
Preparation Products
Tert-Butyl 4-(bromomethyl)phenylcarbamate Suppliers
- Tel
- (+1)-858-699-3322
- Fax
- (+1)-858-876-1948
- info@accelachem.com
- Country
- United States
- ProdList
- 19965
- Advantage
- 58
- Tel
- +1-833-552-7181
- sales@aladdinsci.com
- Country
- United States
- ProdList
- 52927
- Advantage
- 58
View Lastest Price from Tert-Butyl 4-(bromomethyl)phenylcarbamate manufacturers
- Product
- N-Boc-4-(bromomethyl)aniline 239074-27-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- 100kgs/month
- Release date
- 2021-11-20
- Product
- tert-Butyl 4-(bromomethyl)phenylcarbamate 239074-27-2
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.7%
- Supply Ability
- 100 tons
- Release date
- 2022-01-26
- Product
- TERT-BUTYL 4-(BROMOMETHYL)PHENYLCARBAMATE 239074-27-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500kg
- Release date
- 2019-12-26